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Beilstein J. Org. Chem. 2017, 13, 855–862, doi:10.3762/bjoc.13.86
Graphical Abstract
Figure 1: Structures of kipukasins A–J.
Figure 2: Retrosynthetic analysis of kipukasin A.
Scheme 1: Synthesis of 2,4-dimethoxy-6-methylbenzoic chloride. Reagents and conditions: (a) POCl3, DMF, 0 °C ...
Scheme 2: Total synthesis of kipukasin A. Reagents and conditions: (a) I2, acetone, 0 °C to rt, 88%; (b) K2CO3...
Figure 3: X-ray structure of compound 13.